9-Boc-7-oxa-9-azabicyclo [3.3.1] nonan-3-umwe （CAS # 280761-97-9)

Intangiriro

9-Boc-7-oxa-9-azabicyclo [3.3.1] nonan-3-umwe (9-Boc-7-oxa-9-azabicyclo imitungo ikurikira:

1. Kugaragara: 9-Boc-7-oxa-9-azabicyclo [3.3.1] nonan-3-imwe ni ifu ikomeye, ubusanzwe yera cyangwa idafite umweru.

2. Ingingo yo gushonga: Ikigereranyo cyayo cyo gushonga kiri hagati ya 90-95 ° C.

3. Inzira ya molekulari: C14H23NO3

4. Uburemere bwa molekuline: 257.34g / mol

Imikoreshereze nyamukuru yikomatanya niyi ikurikira:

1. Nkurwego rwo hagati muri Synthesis Organic: 9-Boc-7-oxa-9-azabicyclo [3.3.1] nonan-3-imwe ikunze gukoreshwa nkumuhuza muguhuza ibinyabuzima, cyane cyane muguhuza ketone.

2.

Gutegura 9-Boc-7-oxa-9-azabicyclo [3.3.1] nonan-3-imwe muri rusange ikubiyemo intambwe zikurikira:

1. Ubwa mbere, guhera kuri 9-chloro-7-oxa-9-azabicyclo [3.3.1] Nonane, reaction hamwe na BOC (tert-butoxycarbonyl), itsinda rya BOC ryinjijwe muri molekile.

2. Hanyuma, atome ya chlorine ihindurwa mumatsinda ya ketone binyuze muri redox reaction kugirango itange umusaruro ugenewe 9-Boc-7-oxa-9-azabicyclo [3.3.1] nonan-3-imwe.

Mugihe ukoresheje uru ruganda, ugomba kwitondera amakuru yumutekano akurikira:

1.9-boc-7-oxa-9-azabicyclo [3.3.1] nonan-3-imwe irashobora kurakaza uruhu, amaso, hamwe nubuhumekero, bityo rero birakenewe kwambara ibikoresho bikingira bikingira nka gants, ingabo zo mumaso, na gogles mugihe cyo gukora.

2. Irinde guhumeka umukungugu cyangwa gaze yikigo kandi urebe ko ikorerwa ahantu hafite umwuka mwiza.

3. Uru ruganda rugomba kubikwa kure yumuriro na okiside, kandi rukabikwa ahantu humye, hakonje.

4. Mugukoresha no gutunganya uruganda, menya gukurikiza inzira zumutekano zijyanye, gukurikiza amabwiriza yumutekano wa laboratoire hamwe ningamba zo kuyobora.