Lomefloxacin hydrochloride CAS 98079-52-8
Ibyago n'umutekano
Ibimenyetso bya Hazard | Xn - Byangiza |
Kode y'ingaruka | 22 - Byangiza niba byamizwe |
WGK Ubudage | 3 |
RTECS | VB1997500 |
Kode ya HS | 29339900 |
Kwiyemeza ibikubiyemo
Amakuru yemewe Yagenzuwe
gupimwa nubushobozi buhanitse bwa chromatografiya (Rusange 0512).
imiterere ya chromatografique hamwe na sisitemu ikwiranye
silika gel ihujwe na octylsilane nkuzuza; Umuti wa Sodium pentanesulfonate (sodium pentanesulfonate 1.5g, ammonium dihydrogen fosifate 3.0g, amazi 950ml kugirango ushonga, uhindure pH hamwe na acide fosifori, unyunyuze kuri 1000ml n'amazi) -Methanol (65:35) nk'icyiciro kigendanwa, umuvuduko wa 1.2ml kuri umunota, uburebure bwa metero 287mn. Fata sisitemu ikoreshwa igisubizo 20u1 munsi yikintu kijyanye nayo hanyuma uyite muri Chromatograf yumuntu. Igihe cyo kugumana lomefloxacin ni nk'iminota 9, kandi impamyabumenyi yo gutandukanya impinga y’umwanda mugihe cyo kugumana ugereranije na 0.8 nimpinga ya lomefloxacin igomba kuba irenze 2.0, gukemura hagati yimpinga ya lomefloxacin nimpanuka yumwanda mugihe cyo kugumana 1.1 igomba kuzuza ibisabwa.
assay
fata umubare ukwiye wibicuruzwa, gupima neza, wongeyeho gusesagura icyiciro cya mobile hamwe no kugabanuka kwinshi byakozwe muri buri lml irimo nka 0. Igisubizo cya lmg cyakoreshejwe nkigisubizo cyibizamini, naho 20ul yatewe muri chromatografi yamazi neza, na chromatogramu byanditswe. Ikindi kintu cyitwa lomefloxacin cyafashwe kandi kigenwa nuburyo bumwe. Ibiri muri lomefloxacin (C17H19F2N303) murugero byabazwe ahantu hahanamye hakurikijwe uburyo busanzwe bwo hanze.